编者:王红//梁仁校//强根荣
责编:汪靓//宋林青
ISBN：9787122445513
单价：39.8
出版年月：2024-03-01 00:00:00.0
出版社：化学工业出版社
币制：CNY
图书分类：科学技术
分类号： O62-33
语种：CHI
页数：235
装帧：平装
开本：16开
评分：0.0
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目录
Chapter 1 Introduction of Experimental Organic Chemistry
1.1 The Role of Experimental Organic Chemistry
1.2 General Rules for the Organic Chemistry Experiments
1.3 Safety in the Organic Chemistry Laboratory
1.4 Pre-lab Reports.Notebooks and Lab Reports in the Laboratory
1.5 Common Laboratory Glassware and Equipment
1.6 The Literature of Organic Chemistry
1.7 Green Chemistry in the Organic Laboratory
Chapter 2 Basic Operations of Organic Chemistry Experiments
2.1 Heating and Cooling
2.2 Drying Organic Solutions and Solids
2.3 Filtration
2.4 Simple Distillation and Boiling Point
2.5 Fractional Distillation
2.6 Steam Distillation
2.7 Vacuum Distillation
2.8 Extraction and Washing
2.9 Recrystallization
2.10 Sublimation
2.11 Measurement of the Melting Point
2.12 Refluxing
2.13 Stirring Methods
2.14 Water-free and Air-free Operation
2.15 Chromatography Techniques
Chapter 3 Fundamental Experiments
3.1 Unsaturated Hydrocarbons
Exp.1 Preparation of Cyclohexene
Exp.2 Preparation of Phenylacetylene
3.2 Alkyl Halides
Exp.3 Preparation of 1-Bromobutane
Exp.4 Preparation of 2 Chloro 2 methylbutane
3.3 Alcohols，Phenols and Ethers
Exp.5 Preparation of 2-Methyl-2-butanol
Exp.6 Preparation of Triphenylmethanol
Exp.7 Preparation of Di n-butyl Ether
Exp.8 Preparation of Ethyl Phenyl Ether
Exp.9 Preparation of o-tert Butylhydroquinone
3.4 Aldehydes and Ketones
Exp.10 Preparation of Cyclohexanone
Exp.11 Preparation of Acetophenone
Exp.12 Preparation of Benzaldehyde
3.5 Carboxylic Acids
Exp.13 Preparation of Benzoic Acid
Exp.14 Preparation of Cinnamic Acid
Exp.15 Preparation of Hexane-1，6 dionic Acid
3.6 Carboxylic Acid Derivatives
Exp.16 Preparation of Ethyl Acetate
Exp.17 Preparation of nDibutyl Phthalate
3.7 Nitrogen-containing Compounds
Exp.18 Preparation of Acetanilide
Exp.19 Preparation of Methyl Orange
3.8 Heterocyclic Compounds
Exp.20 Preparation of 8-Hydroxyquinoline
Exp.21 Extraction and Separation of Caffeine from Tea Leaves
Chapter 4 Comprehensive Experiments
Exp.1 Preparation of Benzyl Alcohol and Benzoic Acid
Exp.2 Preparation of Benzil and Thin-layer Chromatography
Exp.3 Preparation of Acetylferrocene and Column Chromatography
Exp.4 Preparation of Ethyl Acetoacetate by the Claisen Condensation Reaction
Exp.5 Synthesis and Characterization of Aspirin
Exp.6 Multi-step Synthesis of Sulfanilamide
Exp.7 A Solvent Free Cannizzaro Reaction and Thin-layer Chromatography
Exp.8 Preparation of 4-Vinylbenzoic Acid by a Wittig Reaction
Exp.9 Preparation of Dimedone via the Robinson Annulation
Exp.10 Preparation of Cinnamic Acid by the Knoevenagel Condensation
Exp.11 Microwave assisted Preparation of Benzoic Acid and Ethyl Benzoate
Chapter 5 Experiments from Research and Literature
Exp.1 Synthesis of 3-Substituted Isoindolin-1-ones by Solvent-free Grinding Reaction
Exp.2 Electroorganic Synthesis of Nitriles
Exp.3 Ultrasonic Assisted Green Protocol for the Synthesis of N，N-bis Phenylsulfamide
Exp.4 Clean Synthesis in Water：Uncatalysed Preparation of Ylidenemalononitriles
Exp.5 Transition metal-catalyzed Convenient Synthesis of Internal Alkyne
Exp.6 N-Heterocyclic Carbene Catalyzed Intramolecular Benzoin Condensation to Access 9，10-Phenanthraquinone
Exp.7 Optical Resolution of （★）（S）-Methyl-（S）phenylsulfoximine with （+）-L-Camphorsulfonic Acid
Exp.8 Synthesis of Benzyl Acetate in Room Temperature lonic Liquids
Exp.9 Green Synthesis of 4-Bromoaniline
Exp.10 Pinacol Rearrangement and Photochemical Synthesis of Benzopinacol
Chapter 6 Study Guide of Some Typical Experiments
Exp.1 Preparation of Cyclohexene （Miniscale Reaction）
Exp.2 Preparation of.1
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